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Samples were concentrated to dryness in vacuum before dissolving in 150 L 80% methanol solution, then centrifuged again at 13 500 g and 4C for 10 min, and the supernatant was transferred to a new tube for LC-MS detection

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Safety and efficacy of once-weekly dulaglutide versus sitagliptin after 2 years in metformin-treated patients with type 2 diabetes (AWARD-5): a randomized, phase III study

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